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https://open.uns.ac.rs/handle/123456789/6713
Title: | Reheating of zinc-titanate sintered specimens | Authors: | Labus N. Mentus S. Rakić, Srđan Đurić Z. Vujančević J. Nikolić M. |
Issue Date: | 1-Jan-2015 | Journal: | Science of Sintering | Abstract: | © 2015 International Institute for the Science of Sintering (IISS). All rights reserved. The scope of this work was observing dimensional and heat transfer changes in ZnTiO<inf>3</inf> samples during heating in nitrogen and air atmosphere. Interactions of bulk specimens with gaseous surrounding induce microstructure changes during heating. Sintered ZnTiO<inf>3</inf> nanopowder samples were submitted to subsequent heating. Dilatation curves and thermogravimetric with simultaneous differential thermal analysis TGA/DTA curves were recorded. Reheating was performed in air and nitrogen atmospheres. Reheated samples obtained at different characteristic temperatures in air were analyzed by X-ray diffraction (XRD). Microstructures obtained by scanning electron microscopy (SEM) of reheated sintered samples are presented and compared. Reheating in a different atmosphere induced different microstructures. The goal was indicating possible causes leading to the microstructure changes. | URI: | https://open.uns.ac.rs/handle/123456789/6713 | ISSN: | 0350820X | DOI: | 10.2298/SOS1501071L |
Appears in Collections: | PMF Publikacije/Publications |
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