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https://open.uns.ac.rs/handle/123456789/31409
Title: | Conversion of d́-glucose to methyl α-Daltropyranoside derivatives | Authors: | Djurendic Evgenija Velimirović S. Popsavin Mirjana Popsavin Velimir Miljković D. |
Issue Date: | 1997 | Journal: | Journal of the Serbian Chemical Society | Abstract: | A novel synthesis of methyl α-D-altropyranoside derivatives 5 aid 6 has been achieved starting from methyl α-D-glucopyranoside (1). The action of tosyl chloride in pyridine on compound 1 afforded the 2,6-di-O-tosyl derivative 2 which was further treated with sodium acetate in N,N-dimethylformamide to give the 6-O-acetyl derivative 3. Treatmen of 3 with aqueous potassium hydroxide gave the methyl α-D-altropyranoside (5) which was subsequently acetylated to afford the corresponding peracetylated derivative 6. | URI: | https://open.uns.ac.rs/handle/123456789/31409 | ISSN: | 0352-5139 |
Appears in Collections: | PMF Publikacije/Publications |
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