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Title: | Synthesis and characterization of platinum(IV)-complexes with S-alkyl derivatives of thiosalicylic acid and the crystal structure of the S-butyl derivative of thiosalicylic acid | Authors: | Mijajlovic M. Nikolić, Milica Tomovic D. Bukonjic A. Kocovic A. Jevtic V. Ratkovic Z. Klisurić, Olivera Trifunović, Jasna Radic G. |
Issue Date: | 1-Sep-2017 | Journal: | Serbian Journal of Experimental and Clinical Research | Abstract: | © 2017, University of Kragujevac, Faculty of Science. All rights reserved. New platinum(IV)-complexes with S-alkyl derivatives of thiosalicylic acid (alkyl = benzyl-(L1), methyl-(L2), ethyl-(L3), propyl-(L4), butyl-(L5)) have been synthesized and characterized by microanalysis, infrared spectroscopy, and1H and13C NMR spectroscopy. The bidentate S,O ligand precursor, the S-butyl derivative of thiosalicylic acid (S-bu-thiosal), was prepared, and its crystal structure was determined. Single crystals suitable for X-ray measurements were obtained by slow crystallization from a DMSO-water system. S-bu-thiosal crystallized in a P21/c space group of a monoclinic crystal system with a = 8.0732 (3) Å, b = 19.6769 (4) Å, c = 8.2291 (3) Å and Z = 4. S-bu-thiosal also has a coplanar geometry. | URI: | https://open.uns.ac.rs/handle/123456789/2981 | ISSN: | 18208665 | DOI: | 10.1515/SJECR-2016-0094 |
Appears in Collections: | PMF Publikacije/Publications |
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