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https://open.uns.ac.rs/handle/123456789/14536
Nаziv: | Different intermolecular interactions in azido[2-(diphenylphosphino)benzaldehyde semicarbazonato-κ2P,N1,O]nickel(II) | Аutоri: | Novaković S. Bogdanović G. Brčeski, Ilija Leovac, Vukadin |
Dаtum izdаvаnjа: | 30-јул-2009 | Čаsоpis: | Acta Crystallographica Section C: Crystal Structure Communications | Sažetak: | The title compound, [Ni(C20H17N3OP)(N3)], is the first complex with a semicarbazide-based ligand having a P atom as one of the donors. The influence of the P atom on the deformation of the coordination geometry of the Ni II ion is evident but less expressed than in the cases of complexes with analogous seleno- and thio-semicarbazide ligands. The torsion angles involving the two bonds formed by the P atom within the six-membered chelate ring have the largest values [C - P - Ni - N = 24.3 (2)° and C - C - P - Ni = -24.2 (4)°], suggesting that the P atom considerably influences the conformation of the ring. Two types of N - H⋯N hydrogen bond connect the complex units into chains. © 2009 International Union of Crystallography. | URI: | https://open.uns.ac.rs/handle/123456789/14536 | ISSN: | 01082701 | DOI: | 10.1107/S0108270109021970 |
Nаlаzi sе u kоlеkciјаmа: | Naučne i umetničke publikacije |
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