Please use this identifier to cite or link to this item:
https://open.uns.ac.rs/handle/123456789/18997
DC Field | Value | Language |
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dc.contributor.author | Kragulj Isakovski Marijana | - |
dc.contributor.author | Molnar Jazić Jelena | - |
dc.contributor.author | Maletić Snežana | - |
dc.contributor.author | Tubić Aleksandra | - |
dc.contributor.author | Agbaba Jasmina | - |
dc.contributor.author | Tričković Jelena | - |
dc.contributor.author | Dalmacija Božo | - |
dc.date.accessioned | 2020-12-13T13:15:58Z | - |
dc.date.available | 2020-12-13T13:15:58Z | - |
dc.date.issued | 2018 | - |
dc.identifier.issn | 0949-1775 | - |
dc.identifier.uri | https://open.uns.ac.rs/handle/123456789/18997 | - |
dc.description.abstract | © 2018, Springer-Verlag GmbH Germany, part of Springer Nature. This study investigates measurement procedure validation for the determination of hexachlorobenzene, pentachlorobenzene and trifluralin as priority hazardous pesticides in water with suspended solids < 12 mg/L by liquid–liquid extraction with hexane and gas chromatography with electron capture detector analysis. Two water matrices were used: synthetic matrix and a natural matrix—Danube surface water. Limit of detection was in the range 2.2 ng/L–3.9 ng/L. Trueness expressed as recovery was determined at pesticide concentrations of 20 ng/L and 50 ng/L in both water matrices. The intermediate precision was determined as relative standard deviations (RSD) and represents an agreement between replicates. Trueness was 72 %–121 % with RSD < 20 %. Expanded uncertainty of measurement was similar for all compounds (33.3 %–37.5 %) with a 95 % confidence level, for coverage factor k = 2. The validity of the measurement procedure was confirmed by participation in a PT Scheme with satisfactory |z|-score smaller than 2. Based on these results, it can be concluded that this low-cost measurement procedure is fit for the intended use measurements. | - |
dc.language.iso | en | - |
dc.relation.ispartof | Accreditation and Quality Assurance | - |
dc.source | CRIS UNS | - |
dc.source.uri | http://cris.uns.ac.rs | - |
dc.title | Validation of an in-house measurement procedure for determination of selected priority hazardous substances in water and estimation of measurement uncertainty | - |
dc.type | Journal/Magazine Article | - |
dc.identifier.doi | 10.1007/s00769-018-1334-8 | - |
dc.identifier.scopus | 85049593342 | - |
dc.identifier.url | https://www.cris.uns.ac.rs/record.jsf?recordId=108866&source=BEOPEN&language=en | - |
dc.identifier.url | https://api.elsevier.com/content/abstract/scopus_id/85049593342 | - |
dc.relation.lastpage | 250 | - |
dc.relation.firstpage | 243 | - |
dc.relation.issue | 4 | - |
dc.relation.volume | 23 | - |
dc.identifier.externalcrisreference | (BISIS)108866 | - |
item.fulltext | No Fulltext | - |
item.grantfulltext | none | - |
crisitem.author.dept | Departman za hemiju, biohemiju i zaštitu životne sredine | - |
crisitem.author.dept | Departman za hemiju, biohemiju i zaštitu životne sredine | - |
crisitem.author.dept | Departman za hemiju, biohemiju i zaštitu životne sredine | - |
crisitem.author.dept | Departman za hemiju, biohemiju i zaštitu životne sredine | - |
crisitem.author.dept | Departman za hemiju, biohemiju i zaštitu životne sredine | - |
crisitem.author.dept | Departman za hemiju, biohemiju i zaštitu životne sredine | - |
crisitem.author.dept | Departman za hemiju, biohemiju i zaštitu životne sredine | - |
crisitem.author.orcid | 0000-0002-6880-6735 | - |
crisitem.author.orcid | 0000-0002-8696-7647 | - |
crisitem.author.orcid | 0000-0001-7503-7754 | - |
crisitem.author.orcid | 0000-0002-9915-2885 | - |
crisitem.author.orcid | 0000-0001-5592-9931 | - |
crisitem.author.parentorg | Prirodno-matematički fakultet | - |
crisitem.author.parentorg | Prirodno-matematički fakultet | - |
crisitem.author.parentorg | Prirodno-matematički fakultet | - |
crisitem.author.parentorg | Prirodno-matematički fakultet | - |
crisitem.author.parentorg | Prirodno-matematički fakultet | - |
crisitem.author.parentorg | Prirodno-matematički fakultet | - |
crisitem.author.parentorg | Prirodno-matematički fakultet | - |
Appears in Collections: | PMF Publikacije/Publications |
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